Laboratories
Laboratory Spokesperson: Dr. Stanislaw Skonieczny
Office:LM106A (108)
Telephone:416-978-5297
Email:
List of Experiments 2008
| Lab Period | Title of Experiment | Date |
| 1 | Check-in. Solubility and Crystallization. Melting Points |
January 11 |
| 2 | Extraction: Part 1 (Microscale); Drawing of Chemical Formulae |
January 18 |
| 3 | Infrared and NMR Spectroscopy |
January 25 |
| 4 | Reduction of Conjugated Ketones with NaBH4 |
February 1 |
| 5 | Multistep Synthesis 1. Part A: Reduction of 4-Nitrophenol |
February 8 |
| 6 | Multistep Synthesis 1. Part B: Acetylation of 4-Aminophenol |
February 15 |
| 7 | Multistep Synthesis 1. Part C: Etherification of 4-Hydroxyacetanilide |
March 1 |
| 8 | Multistep Synthesis 2. Part A: Synthesis of 4-Bromoacetanilide |
March 8 |
| 9 | Multistep Synthesis 2. Part B: Synthesis of 4-Bromo-2-chloroacetanilide |
March 15 |
| 10 | Multistep Synthesis 2. Part C: Hydrolysis of 4-Bromo-2-chloroacetanilide |
March 29 |
| 11 | Multistep Synthesis 2. Part D: Synthesis of 1-Bromo-3-chlorobenzene |
April 4 |
Notes:
1. The lab starts on the hour (9:00 a.m. sharp), not at 9:10 a.m.
2. There will a quiz during first several minutes of the lab (including one on January 11).
..... If you are late, you will not be allowed to write a quiz.
3. If you are late by more than 15 minutes, you will not be allowed to perform the experiment.
4. There are no make-ups. The labs are only on Friday mornings every week.
5. Bring your safety glasses (goggles), lab coat and a note book on January 11.
Laboratory Notes:
Please read these notes for preparation for the laboratories.
Site design by Robert Batey.
© Department of Chemistry, The University of Toronto